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1 article(s) from Comoretto, Davide

Photocatalyzed synthesis of isochromanones and isobenzofuranones under batch and flow conditions

Manuel Anselmo,
Lisa Moni,
Hossny Ismail,
Davide Comoretto,
Renata Riva and
Andrea Basso

Beilstein J. Org. Chem. 2017, 13, 1456–1462, doi:10.3762/bjoc.13.143

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Graphical Abstract

Scheme 1: Photo-Meerwein reaction leading to amides.

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Figure 1: Products detected in the reaction mixtures during attempts to intercept the radical/cationic interm...

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Scheme 2: Reaction of o-alkoxycarbonyldiazonium salts with alkenes under Ru-photocatalyzed conditions.

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Scheme 3: Proposed mechanism for the reaction of diazonium salt 2h with methyl methacrylate (3a).

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Scheme 4: Reaction of 2-aminocarbonyldiazonium salt 2i with styrene (3b).

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Figure 2: The meso-flow apparatus assembled in-house. The components are shown on the left, while the operati...

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Scheme 5: Reaction of diazonium salts 11 with styrenes 12. The nucleophilic attack to intermediate A is given...

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Scheme 6: Proposed mechanism for the formation of benzo[e][1,3]oxazepin-1(5H)-one 14.

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Scheme 7: Investigation of the selectivity of the photochemically induced cyclization.

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Published 25 Jul 2017

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